CHEM 242 Laboratory Schedule

Spring 2013

Week	Experiment Name	Prelab Reading
Jan 7-11	Spectroscopy (handout) Instructions for Printing Spectra Spectroscopy unknown	Chapters 15 & 16
Jan. 14-18	Spectroscopy Introductory Material	Chapters 15 & 16
Jan. 22-25 Jan. 28	Extraction (handout) Extraction & crystallization, NMR data	Handout Techniques 11.1-11.4, 11.6, 10.1-10.2, 10.4-10.6
Jan. 29-Feb. 1 Feb. 4	Crystallization and Extraction, cont’d	Techniques 14, 15.1-15.5, 15.8
Feb. 5-8 Feb. 11	Kinetics (handout)	Handout
Feb.12-15	No labs (week of Assessment Day)
Feb. 18-22	Distillation (handout)	Handout Techniques 7,13.1-13.3b,13.4,13.8
Feb. 25-Mar.1	Gas chromatography of distillation products Synthesis of p-nitroacetanilide (handout)	pp 219-220, Technique 19 Handout
Mar. 4-8	SPRING BREAK
Mar. 11-15	Midterm exam TLC of analgesic drugs (handout)	Handout Techniques 17
Mar. 18-22	Dehydration of an alcohol (handout)	Handout Techniques 13.6, 12
Mar. 25-29	Synthesis: Metalation (handout)	Handout
April 1-5	Synthesis of a Gemini amphiphile (handout) Multi-step Synthesis: Dilantin (handout)	Handouts
April 8-12	Multi-step Synthesis: Dilantin (NMR data)	Handout, Technique 7.1
April 15-19	Multi-step Synthesis: Dilantin
April 22-26	Cleanup and final exam